Evaluation of the uncertainty associated with sample holders in NAA measurements in LAN/IPEN

Autores/as

  • Guilherme Soares Zahn Instituto de Pesquisas Energéticas e Nucleares - IPEN-CNEN/SP
  • Regina Beck Ticianelli Instituto de Pesquisas Energéticas e Nucleares - IPEN-CNEN/SP
  • Mitiko Saiki Instituto de Pesquisas Energéticas e Nucleares - IPEN-CNEN/SP
  • Frederico Antonio Genezini Instituto de Pesquisas Energéticas e Nucleares - IPEN-CNEN/SP

DOI:

https://doi.org/10.15392/bjrs.v7i2A.676

Palabras clave:

NAA, uncertainty, sample holder

Resumen

In IPEN’s Neutron Activation Laboratory (LAN/IPEN), thin stainless steel sample holders are used for gamma spectrometry in NAA measurements. This material is very practical, but its chemical composition may be troublesome, as it presents large amounts of elements with intermediate atomic number, with attenuation factors for low-energy gamma-rays that must not be neglected. In this study, count rates obtained using different sample holders were compared. To accomplish that, an Am-241 source, with 59-keV gamma emission, was used so that low-energy gamma attenuation differences can be determined. Moreover, in order to study the energy dependence of these differences, a Ho-166m source was also used. From these results, it was possible to analyze the experimental error associated to the variations between sample holders, with the aim of introducing an addictive term to the uncertainty analysis of comparative Neutron Activation Analysis results.

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Biografía del autor/a

  • Guilherme Soares Zahn, Instituto de Pesquisas Energéticas e Nucleares - IPEN-CNEN/SP
    Centro do Reator de Pesquisas - CRPq
  • Regina Beck Ticianelli, Instituto de Pesquisas Energéticas e Nucleares - IPEN-CNEN/SP
    Centro do Reator de Pesquisas - CRPq
  • Mitiko Saiki, Instituto de Pesquisas Energéticas e Nucleares - IPEN-CNEN/SP
    Centro do Reator de Pesquisas - CRPq
  • Frederico Antonio Genezini, Instituto de Pesquisas Energéticas e Nucleares - IPEN-CNEN/SP
    Centro do Reator de Pesquisas - CRPq

Referencias

JCGM-Joint Committee for Guides in Metrology, JCGM 100:2008 - Evaluation of measurement data Guide to the expression of uncertainty in measurement, JCGM, 2008.

LOVELAND, W. D.; MORRISSEY, D. J.; SEABORG, G. T. Modern Nuclear Chemistry, Hoboken, , John Wiley & Sons, Inc, 2006.

ZAHN, G. S.; TICIANELLI, R. B.; LANGE, C. N.; FÁVARO, D. I. T.; FIGUEIREDO, A. M. G. Uncertainty Analysis in Comparative NAA Applied to Geological and Biological Matrices, In: IN-TERNATIONAL NUCLEAR ATLANTIC CONFERENCE, 2015, São Paulo. Annals… São Paulo: Comissão Nacional de Energia Nuclear, 2015.

WEIZHI, T.; BANGFA, N.; PINGSHENG, W.; LEI, C.; YANGMEI Z. Metrological role of neu-tron activation analysis. IA. Inherent characteristics of relative INAA as a primary ratio method of measurement, Accreditation and Quality Assurance, v. 6, p.488–492, 2001.

GREENBERG, R.; BODE, P.; DE NADAI FERNANDES, E. A. Neutron activation analysis: A primary method of measurement, Spectrochimica Acta Part B: Atomic Spectroscopy, v.66, p.193–241, 2011.

LNHB-Laboratoire National Henri Becquerel Table de Radionocléides, 2017 Available at: <http://www.nucleide.org/DDEP_WG/DDEPdata.htm>. Last accessed: 22-Nov-2017.

KNOLL, G. F. Radiation Detection and Measurement, Hoboken

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Publicado

2019-02-20

Número

Sección

The Meeting on Nuclear Applications (ENAN)

Cómo citar

Evaluation of the uncertainty associated with sample holders in NAA measurements in LAN/IPEN. Brazilian Journal of Radiation Sciences (BJRS), Rio de Janeiro, Brazil, v. 7, n. 2A (Suppl.), 2019. DOI: 10.15392/bjrs.v7i2A.676. Disponível em: https://bjrs.org.br/revista/index.php/REVISTA/article/view/676. Acesso em: 16 jul. 2025.