Preparation and Thermoluminescence Properties of Polycrystalline Na2SO4/SiO2 composite
DOI:
https://doi.org/10.15392/2319-0612.2024.2322Keywords:
TLD, Geode, SilicaAbstract
A sodium sulphate/silica (Na2SO4/SiO2) composite was prepared by a sol-gel procedure using a geode as the silica source. The prepared sample was characterized by XRD, XRF and IR techniques. The Na2SO4/SiO2 has an orthorhombic phase, and an average crystalline size is about 51 nm. Thermoluminescence characteristics of Na2SO4/SiO2 were studied at different parameters. The glow curve resulting from Na2SO4/SiO2 showed one clear peak between 150 oC to 200 oC, depending on the energy. The general peak structure of the TL glow curve remains unchanged as a result of repeated cycles of irradiation at various X–ray energies, and exhibits good linearity over the used exposure. There were no significant changes in the TL reading after ten times of reuse, and the fading was observed at 56% after 15 days of irradiation and after one month about 82.3% of the TL signal was lost, and the value of Zeff of Na2SO4/SiO2 was found to be 13.56.
- Views: 164
- PDF Downloads: 94
- XML Downloads: 17
Downloads
References
KRON, T. Thermoluminescence dosimetry and its applications in medicine-Part 1: Physics, materials and equipment. Australasian Physical and Engineering Sciences in Medicine. 1994, 17, 175–199.
MOSCOVITCH, M.; JOHN, T.J.; CASSATA, J. R.; BLAKE, P. K.; ROTUNDA, J. E.; RAMLO, M.; VELBECK, K.J.; LUO, L. Z. The application of LiF:Mg,Cu,P to large scale personnel dosimetry: Current status and future directions. Radiation Protection Dosimetry. 2006, 119, 248–254. DOI: https://doi.org/10.1093/rpd/nci692
CHAND, S.; MEHRA, R.; CHOPRA, V. Recent developments in phosphate materials for their thermoluminescence dosimeter (TLD) applications. Luminescence 2021, 36, 1808–1817. DOI: https://doi.org/10.1002/bio.3960
Preusser, F.; Chithambo, M. L.; Götte, T.; Martini, M.; Ramseyer, K.; Sendezera, E. J.; Susino, G. J.; Wintle, A.G. Quartz as a natural luminescence dosimeter. Earth Science Reviews. 2009, 97, 184–214. DOI: https://doi.org/10.1016/j.earscirev.2009.09.006
Thamóné Bozsó, E.; Füri, J.; Kovács István, J.; Biró, T.; Király, E.; Nagy, A.; Törökné Sinka, M.; Kónya, P.; Mészárosné Turi, J.; Vígh, C. Characteristics of quartz separates of different formations in Hungary from the aspect of osl dating. Foldt. Kozlony 2020, 150, 61. DOI: https://doi.org/10.23928/foldt.kozl.2020.150.1.61
Bailiff, I. K.; Stepanenko, V. F.; Göksu, H.Y.; Bøtter-Jensen, L.; Brodski, L.; Chumak, V.; Correcher, V.; Delgado, A.; Golikov, V.; Jungner, H.; et al. Comparison of retrospective luminescence dosimetry with computational modeling in two highly contaminated settlements downwind of the chernobyl NPP. Health Physics. 2004, 86, 25–41. DOI: https://doi.org/10.1097/00004032-200401000-00006
BENEITEZ, P.; CORRECHER, V.; MILLAN, A.; CALDERON, T. Thermoluminescence analysis for testing the irradiation of spices. Journal of Radioanalytical and Nuclear Chemistry. 1994, 185, 401–410. DOI: https://doi.org/10.1007/BF02041311
ELDER. J. P., Thermal energy storage materials-a DSC study, Thermochimica Acta, vol. 36, no. 1, 1980. pp. 67–77. DOI: https://doi.org/10.1016/0040-6031(80)80110-9
WIEDEMANN. H. G., Thermal studies on thenardite, Thermochimica Acta, vol. 50, no. 1–3, 1981. pp. 17–29. DOI: https://doi.org/10.1016/0040-6031(81)85039-3
VIDYA .Y. S.; LAKSHMINARASAPPA .B. N. Preparation, Characterization, and Luminescence Properties of Orthorhombic Sodium Sulphate, Physics Research International Volume 2013, Article ID 641631, 7 pages. DOI: https://doi.org/10.1155/2013/641631
WANG, W. L. ; YANG, X. X. ; FANG, Y.T. ; DING, J., Preparation and performance of form-stable polyethylene glycol/silicon dioxide composites as solid-liquid phase change materials, Applied Energy., 86, 2009.170 -174 DOI: https://doi.org/10.1016/j.apenergy.2007.12.003
ARUN KUMAR D. ; MERLINE SHYLA J. ; FRANCIS P. XAVIER. Synthesis and characterization of TiO2/SiO2 nano composites for solar cell applications, Applied Nanoscience 2, 2012. pp. 429-436. DOI: https://doi.org/10.1007/s13204-012-0060-5
ZHANG Y. JIN S. ; YANG Y. ; CHUNSHENG Y. Annealing effects on the phase and microstructure transformations of nanocrystalline (ZrO2)1−x(Sc2O3)x (x=0.02-0.16) thin films deposited by sol-gel method. Solid State Communications. 2002 .122 7-8, 439 444. DOI: https://doi.org/10.1016/S0038-1098(02)00152-7
RAVIKUMAR, N. R.; ARUN KUMAR, B. S.; PANIGRAHI, U. ; DHUSOODANAN, C. B. ; PALAN, AND S. K. OMANWAR. Spectral and Thermoluminescence Characteristics of High Gamma Dose Irradiated Dy:LiKB4O7 Single Crystals. Nuclear Instruments and Methods in Physics Research, Section B: Beam Interactions with Materials and Atoms 436(September) 2018 :203–10. DOI: https://doi.org/10.1016/j.nimb.2018.09.040
CHEN, R.; PAGONIS, V.; LAWLESS, J. L. Evaluated thermoluminescence trapping parameters-What do they really mean? Radiation Measurements. 2016, 91, 21–27. DOI: https://doi.org/10.1016/j.radmeas.2016.04.006
MAGHARBI. M. ; ARAFAH D. E. ; Sensitization of the thermoluminescence response of CaF2 phosphors, Physica Status Solidi (A), vol. 195, no. 2, 2003. pp. 459–467. DOI: https://doi.org/10.1002/pssa.200305938
HAMZAH, S. A.; SAEED M. A.; WAGIRAN. H.; AND HASHIM. I. H.; Thermoluminescence (TL) Dosimeter of Dysprosium Doped Strontium Borate Glass for Different Glass Modifiers (Na, Li, Ca) Subjected from 1 to 9 Gy Doses. EPJ Web of Conferences 2017.156:1–6. DOI: https://doi.org/10.1051/epjconf/201715600007
MOHAMMED BAHRA,; JAAFAR. M. S.; AND WAGIRAN. H.; Thermoluminescence Dosimetry Properties and Kinetic Parameters of Zinc Borate Silica Glass Doped with Cu2O and Co-Doped with SnO2. Journal of Luminescence 204 (December 2017):375–81 DOI: https://doi.org/10.1016/j.jlumin.2018.08.020
FURETTA, C.; Handbook of thermoluminescence: 2nd ed. Singapore: World Scientific, 2010. DOI: https://doi.org/10.1142/7187
Published
How to Cite
Issue
Section
License
Copyright (c) 2024 Brazilian Journal of Radiation Sciences
This work is licensed under a Creative Commons Attribution 4.0 International License.
Licensing: The BJRS articles are licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made. The images or other third party material in this article are included in the article’s Creative Commons license, unless indicated otherwise in a credit line to the material. If material is not included in the article’s Creative Commons license and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this license, visit http://creativecommons.org/licenses/by/4.0/
