Calibration Of The Short Irradiation Facility For k0 - NAA Implementation At The IEA-R1 Reactor
DOI:
https://doi.org/10.15392/bjrs.v9i1A.1570Keywords:
k0 methodAbstract
The short irradiation facility of the IEA-R1 nuclear research reactor at IPEN, São Paulo, Brazil, has been used for short irradiation of samples for the purpose of determining the concentration of elements of these samples through the use of the instrumental neutron activation analysis technique. With the aim of implementing the k0-NAA method at the Neutron Activation Analysis Laboratory (LAN), the reactor parameters a and f were obtained using the bare triple method. In this method, a set of three neutron flux monitors were irradiated without Cd-cover. The efficiency curve of the gamma-ray spectrometer used was determined by measuring calibrated radioactive sources at the commonly used counting geometries. The results for the parameters a and f were respectively 0.0384±0.0016 and 35.67±0.26. This value of f shows that the neutrons in the irradiation position are well thermalized.The variation of these parameters was studied with time and the reproducibility was verified.Downloads
References
SIMONITS A, DE CORTE F, HOSTE J, ``Single-Comparator Methods in Reactor Neutron Activation Analysis", Journal of Radioanalytical and Nuclear Chemistry, 24, pp. 31--46, (1975).
LANGE, C. N.; CAMARGO, I. M. C.; FIGUEIREDO, A. M. G. M; CASTRO, L.; VASCONCELLOS, M. B. A.; TICIANELLI, R. B., ``A Brazilian coal fly ash as a potential source of rare earth elements", Journal of Radioanalytical and Nuclear Chemistry, 311, pp. 1235--1241, (2017).
FAVARO, D. I. T.; ROCHA, F. R.; ANGELINI, M.; HENRIQUES, H. R. A.; SOARES, J. S.; SILVA, P. S. C.; OLIVIERA, S. M. B., ``Metal and trace element assessments of bottom sediments from medium Tietê River basin, Sao Paulo State, Brazil: part II", Journal of Radioanalytical and Nuclear Chemistry, 316, pp. 805--818, (2018).
CARVALHO, P. R.; MUNITA, C. S.; NEVES, E. G.; ZIMPEL, C. A., ``Chemical characterization of ancient pottery from the south-west Amazonia using instrumental neutron activation analysis", Brazilian Journal Of Radiation Sciences, 7, pp. 1--14, (2019).
SILVA, R. C. A.; SAIKI, M.; MOREIRA, E. G.; OLIVEIRA, P. T. M. S., ``The great egret (Ardea alba) as a bioindicator of trace element contamination in the São Paulo Metropolitan Region, Brazil", Journal of Radioanalytical and Nuclear Chemistry, 315, pp. 447--458, (2018).
SALES, T.N.S., BOSCH-SANTOS, B., SAIKI, M., BURIMOVA, A., PEREIRA, L.F.D., SAXENA, R.N., CARBONARI, A.W., ``Low temperature synthesis of pure and Fe-doped HfSiO4: Determination of Si and Fe fractions by neutron activation analysis", Radiation Physics and Chemistry, 155, pp. 287--290, (2019).
SAIKI, M.; SOARES, M. A. B.; ADACHI, E. M., ``INAA of enamel and dentine samples of a group of children and adults: A comparative study", Journal of Radioanalytical and Nuclear Chemistry, 276, pp. 49--52, (2008).
DE CORTE, F. The k00-Standardization Method: A Move to the Optimisation of Neutron Activation Analysis, Rijksuniversiteit Gent, Faculteit Van de Wetenschappen, Gent & Belgium (1986).
DE CORTE F, MOENS L, SIMONITS A, DE WISPERLAERE A, HOSTE J., ``k0 Method", Journal of Radioanalytical and Nuclear Chemistry, 52, pp. 295, (1979).
DE CORTE F, SIMONITS A, ``Recommended nuclear data for use in the k0 standardization of neutron activation analysis", At. Data Nucl. Data Tables, 85, pp. 47--67, (2003).
MIRSHAWKA, VICTOR, ``Cálculo Numérico ",São Paulo , 3 ed. , Nobel, 1983
SEMMLER R, FIGUEIREDO A. M. G., FLORES J. P. O., GONÇALEZ O. L., FEDERICO C. A., ``Characterization of neutron spectrum at the short irradiation facility of the IEA-R1 reactor using HOgdahl formalism for the k0 standardization", XXV Reunião de Trabalho sobre Física Nuclear no Brasil, Maresias, SP from 2 to 6 of september, 2012
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