Preliminary chemical studies at the jericho archaeological site
DOI:
https://doi.org/10.15392/bjrs.v9i1A.1319Keywords:
archaeometry, INAA, pottery, tell es-SultanAbstract
This study measured the chemical composition of 45 ceramic samples from the Jericho archaeological site, Palestine, by means of instrumental neutron activation analysis (INAA). The mass fraction of Na, K, La, Sm, Yb, Lu, U, Sc, Cr, Fe, Co, Zn, Rb, Cs, Ce, Eu, Hf and Th was determined with the purpose to detect the presence of ceramic groupings based on their composition. The analytical method is appropriate for this type of study because it is a non-destructive technique with high sensitivity, accuracy and precision, and determines chemical elements in trace and ultra-trace levels. These characteristics are essential to study small concentration variations. Initially the mass fractions were normalized to compensate for the large difference in magnitude among elements determined in percentage and trace level. Subsequently, the dataset was interpreted through cluster and discriminant analysis. The results showed the existence of three different chemical groups.
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References
AMORIM, L. B. Cerâmica marajoara: a comunicação do silêncio. Museu Paraense Emilio Goeldi, Belém – Pará, 2010.
POLLARD, A.M. Archaeometry 50th Anniversary Issue Editorial. Archaeometry, v. 50(2), p. 191-193, 2008.
ADAMS, W.Y.; ADAMS, E.W. Archaeological typology and practical reality: a dialectical approach to artifact classification and sorting, Cambridge University Press, Cambridge – England, 1991.
SANTOS, J.O.; MUNITA, C.S.; SOARES, E.A.A. Provenance studies in Amazon basin by means of chemical composition obtained by INAA, Journal of Radioanalytical and Nuclear Chemistry, v. 306, p. 713-719, 2015.
ROTUNNO, T.; SABBATINI, L.; CORRENTE, M. A provenance study of pottery from archaeological site near Canosa, Puglia (Italy), Archaeometry, v. 39, p. 343-354, 1997.
CALPARSORO, E.; MAGUREGUI, M.; MORILLAS, H.; ARANA, G.; INANEZ, J.G. Non-destructive screening methodology based on ED-XRF for the classification of medieval and post-medieval archaeological ceramics, Ceramics International, v. 45, no. 8, p. 10672-10683, 2019.
MUNITA, C. S.; CARVALHO, P.R. Grupo de estudos arqueométricos do IPEN-CNEN/SP, Cadernos do CEOM, v. 28, p.53-59, 2015.
MUNITA, C.S. Contribuição da análise por ativação com nêutrons a estudos arqueométricos: estudo de caso, Canindé, v. 6, p. 159-181, 2005.
HAZENFRATZ, R.; MUNITA, C.S.; GLASCOCK, M.D.; NEVES, E.G. Study of exchange networks between two Amazon archaeological sites by INAA, Journal of Radioanalytical and Nuclear Chemistry, v. 309, p. 195-205, 2016.
MUNITA, C.S.; PAIVA, R.P.; MOMOSE, E.F.; OLIVEIRA, P.M.S. Chemical characterization of Brazilian prehistoric ceramics by INAA, In: Nuclear Analytical Techniques in Archaeological Investigations, IAEA Technical Report Series, v. 416, Chapter 5, p. 89-97, 2003.
RIBEIRO, R.B. Caracterização Físico-Química da Cerâmica do Sítio Arqueológico São Paulo II, Dissertação de Mestrado, Instituto de Pesquisas Energéticas e Nucleares, Universidade de São Paulo, 2013.
MUNITA, C.S.; PAIVA, R.P.; ALVES, M.A.; OLIVEIRA, P.M.S.; MOMOSE, E.F. Provenance study of archaeological ceramics. Journal of Trace Microprobe Techniques, v. 21, p. 697-706, 2003.
NIGRO, L.; MONTANARI, D.; MURA, F.; YASINE, J.; RINALDI, T. A hoard of Nilotic nacreous shells from Egypt to Jericho (Early Bronze II, 3000-2800 BCE): Their finding, content and historical archaeological implications, Palestine Exploration Quarterly, v. 150, p. 110-125, 2018.
NIGRO, L.; CALCAGNILE, L.; YASIN, J.; GALLO, E.; QUARTA, G. Jericho and the chronology of Palestine in the Early Bronze Age: A Radiometric Re-assessment, Radiocarbon, v. 61(1), p. 211-241, 2019.
HAZENFRATZ, R.; MONGELÓ, G.; MUNITA, C. S.; NEVES, E. G. Comparison of INAA elemental composition data between Lago Grande and Osvaldo archaeological sites in the central Amazon: a first perspective, Journal of Radioanalytical and Nuclear Chemistry, v. 291, p. 43-48, 2012.
MUNITA, C. S.; CARVALHO, P.R.; OLIVEIRA, C.A.; AMARAL, A.M.; SULLASI, H.L. Estudo da mobilidade logística a partir da caracterização química da cerâmica do Sítio Capim em Araripina, Pernambuco, Brasil, Cadernos do Lepaarq, v. XV, n.30, p. 179-190, Jul-Dez, 2018.
GLASCOCK, M.D.; BRASWELL, G.E.; COBEAN, R.H. A systematic approach to obsidian source characterization, In: Archaeological Obsidian Studies: Method and Theory, Shackley, M.S., Ed., Advances in Archaeological and Museum Science, Plenum Press: New York, v. 3, p. 15-65, 1998.
International Soil-Analytical Exchange, ISE-2015-1, Wageningen Evaluation Programs for Analytical Laboratories. Quaterly Report 2015-1, January-March, Wageningen University, Netherland, 2015.
BISHOP, R. L.; CANOUTS, V.; CROWN, P. L.; DE ATLEY, S. P. Sensitivity, precision and accuracy: their roles in ceramic compositional data bases, American Antiquity, v. 55, no. 3, p. 537–546, 1990.
GLASCOCK, M.D. Characterization of archaeological ceramics at MURR by NAA and Multivariate Statistics, Chemical characterization of Ceramic Paste in Archaeology, Prehistory Press, New York, section1: p. 11-26, 1992.
ATTAS, M.; FOSSEY, J. M.; YAFFE, Y. Corrections for Drill-bit Contamination in Sampling Ancient Pottery for Neutron Activation Analysis, Archaeometry, v. 26, p. 104-107, 1984.
StatSoft, Inc. STATISTICA (data analysis software system), version 8.0, 2007. Available at: .
CARVALHO, P.R.; MUNITA, C.S.; LAPOLLI, A.L. Validity studies among hierarchical methods of cluster analysis using cophenetic correlation coefficient, Brazil Journal of Radiation Sciences, v. 7 (2A), 2019. Available at: <https://www.bjrs.org.br/revista/index.php/REVISTA/article/view/668/428>. Last accessed: 10 March 2019.
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