Elementary characterization of Ti metal alloys used in implant dentistry
DOI:
https://doi.org/10.15392/bjrs.v7i2A.545Keywords:
Dental implants, XRF, Alloy metalAbstract
The main goal of present work is analytical characterization of standard dental implants broadly used by Brazilian dentists. An ideal biological alloy for dental implants must have very high biocompatibility, which means that such material should not provoke any serious adverse tissue response. Dental implants are generally marketed as commercially pure titanium (TiCP) due to their excellent mechanical and physical properties. However, sometimes other alloys are employed and consequently it is essential to study the chemical elements present in those alloys that could bring prejudice for the health. Present work investigated TiCP metal alloys used for dental implant manufacturing and evaluated the presence of elements. For alloy characterization and identification of elements it was used EDXRF technique. This method allows to perform the qualitative and quantitative analysis of the materials using the spectra of the characteristic X-rays emitted by the elements present in the metal samples. The experimental setup was based on two X- ray tubes, Mini X model with Ag and Au targets and X-123SDD detector (AMPTEK) and a 0.5 mm Cu collimator, developed due to specific sample geometrical and topography characteristics. Obtained results showed that implant alloys are not exactly TiCP but were manufactured using Ti-Al-V alloy, which contained Fe, Ni, Cu and Zn. The presence of such metals as Al and V in all studied samples shows very clear that studied implants were not manufactured from TiCP alloy. Moreover, according to the American Society for Testing and Materials (ASTM), these elements should not be present in TiCP.
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HADDAD, M.F.; PELLIZZER, E.P.; MAZARO, J.V.Q.; VERRI, F.R.; FALCÓN-ANTENUCCI, R.M. Conceitos básicos para a reabilitação oral por meio de implantes osse-ointegrados - parte I: influência do diâmetro e do comprimento. Revista Odontológica de Araçatuba, v.290, n.1, pp. 30-37, 2008.
AOKI, T.; OKAFOR, I.C.I.; WATANABE, I.; HATTORI, M.; ODA, Y.; OKABE, T. Mechanical properties of cast Ti-6Al-4V-XCu alloys. Journal of Oral Rehabilitation, v. 31, n.11, pp.1109-1114, 2004.
LEYENS, C.; PETERS, M. Titanium and titanium alloys: fundamentals and applica-tions, Weinheim, WILEY-VCH Verlag GmbH & Co. KGaA, 2003.
LIU, P.; YAO,Y.N.; WU, S.D.; DONGA, H-J.; FENGA, G-C.; YUANA, X-Y. The effica-cy of deferiprone on tissues aluminumremoval and copper, zinc, manganese level in rabbits. J. Inorg Biochem, v. 99, n.8, pp. 1733-1737, 2005.
WATAHA, J. C. Biocompatibility of dental casting alloys: a review. J Prosthet Dent, v.83, n.2, pp. 223-234, 2000.
PALMQUIST, A.; OMAR, M.O.; ESPOSITO, M.; LAUSMA, A. J.; THOMSEN, P. Tita-nium oral implants: surface characteristics, interface biology and clinical outcome. J. R. Soc. Interface, v.7, pp.515-527, 2010.
ANVISA - Agencia Nacional de Vigilância Sanitária. Manual do usuário da resolução- RDC nº 185/2001: orientações sobre registro, cadastramento, alterações, revalidações e cancelamento do registro de produtos médicos. Brasília, DF, Brazil, 2001. Available at: <http://200.189.113.52/ftp/Visa/correlatos/ManualdoUsuariodaRDC185.pdf>. Lasted acessed: Jun. 2014.
MISCH, C. E. Implante Odontológico Contemporâneo, 3ª ed. Rio de Janeiro: Elsevier, 2009.
GRIEKEN, R. E. V.; MARCOWICZ, A. A. Handbook of X-Ray Spectrometry, 2rd ed. New York: Marcel Dekker, 2002.
ASTM - American Society for Testing and Materials. Designation F67–06: Standard Spec-ification for Unalloyed Titanium, for Surgical Implant Applications. ASTM Report UNS R50250, UNS R50400, UNS R50550, UNS R50700, West Conshohocken: ASTM, 2006.
ASTM - American Society for Testing and Materials. Designation F67-13: Standard Speci-fication for Unalloyed Titanium, for Surgical Implant Applications. Report UNSR50250, UNS R50400, UNS R50550, UNS R50700, West Conshohocken: ASTM, 2013.
ASM Handbook, Properties and Selection: Nonferrous Alloys and Special-Purpose Ma-terials, v.2, 10rd ed. United States of America: ASM International Handbook Committee, 1990.
NIST - National Institute of Standards and Technology. unalloyed titanium A. Report SRM 650, Gaithersburg: NIST,1985.
NIST - National Institute of Standards and Technology. titanium Alloy 6Al-4V. Report SRM 654b, Gaithersburg: NIST, 2013.
NIST - National Institute of Standards and Technology. Ti-Al-V SRM 173c. Report SRM 173c, Gaithersburg: NIST, 2016.
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